NMR experiment setup scripts for VNMRJ

From Wiki

Share/Save/Bookmark
Jump to: navigation, search

2D [15N,1H] HSQC

  • HTP_NHSQC_long - 256 complex points in t1, 8 scans, 32 dummy scans
  • HTP_NHSQC_short - 60 ms t1,max, 4 scans
  • HTP_NHSQC_wide - 40 ms t1,max, 4 scans, 15N spectral width 3 times the probefile value


2D [13C,1H] HSQC

  • HTP_CaliHSQC - gradient/sensitivy enhanced, 13C spectral width 80 ppm, 7 ms t1,max, 4 scans
  • HTP_CaroHSQC - gradient/sensitivy enhanced, 13C spectral width 40 ppm, 5 ms t1,max, 8 scans
  • HTP_ctCaliHSQC - gradient/sensitivy enhanced, 13C spectral width 80 ppm, 27 ms constant-time delay
  • HTP_ctCaroHSQC - gradient/sensitivy enhanced, 13C spectral width 40 ppm, 16 ms constant-time delay
  • gChsqc_methyl - 28 ms constant-time delay, optimized for methyl groups


3D Triple-resonance

  • HTP_HNCO_3D - 13C spectral width 20 ppm, 7 ms t1,max, ni2 is 32 or max, 2 scans
  • HTP_HNCACO_3D - 13C spectral width 20 ppm, 7 ms t1,max, ni2 is 32 or max, 2 scans
  • HTP_CBCACONH_3D - 13C spectral width 80 ppm, 6 ms t1,max or max allowed, ni2 is 32 or max, 2 scans
  • HTP_HNCACB_3D - 13C spectral width 80 ppm, 6 ms t1,max, ni2 is 32 or max, 2 scans
  • HTP_HBHACONH_3D - 1Hab spectral width 9 ppm, 15 ms t1,max, ni2 is 32 or max, 2 scans
  • HTP_HCCH_COSY_3D -
  • HTP_HCCH_TOCSY_3D
Personal tools